Characterization of block oligomeric peptides by 2D 1H NMR

Mark I L Liff, Ping chiang Lyu, Neville R. Kallenbach

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

Block copolymers are normally expected to present assignment problems due to degeneracy of the resonances. The authors show here that these difficulties can be circumvented for block oligomeric peptides by tracing connectivities through all possible combinations and use of the DQF-COSY experiment. The assignment of a number of resonances in the 1H NMR spectrum of the parent block oligomer of this series is described.

Original languageEnglish (US)
Title of host publicationAmerican Chemical Society, Polymer Preprints, Division of Polymer Chemistry
PublisherPubl by ACS
Pages139-140
Number of pages2
Volume31
Edition1
StatePublished - Apr 1990
EventPapers Presented at the Boston, Massachusetts Meeting of ACS 1989 - Boston, MA, USA
Duration: Apr 22 1989Apr 27 1989

Other

OtherPapers Presented at the Boston, Massachusetts Meeting of ACS 1989
CityBoston, MA, USA
Period4/22/894/27/89

Fingerprint

Peptides
Nuclear magnetic resonance
Oligomers
Block copolymers
Experiments

ASJC Scopus subject areas

  • Polymers and Plastics

Cite this

Liff, M. I. L., Lyu, P. C., & Kallenbach, N. R. (1990). Characterization of block oligomeric peptides by 2D 1H NMR. In American Chemical Society, Polymer Preprints, Division of Polymer Chemistry (1 ed., Vol. 31, pp. 139-140). Publ by ACS.

Characterization of block oligomeric peptides by 2D 1H NMR. / Liff, Mark I L; Lyu, Ping chiang; Kallenbach, Neville R.

American Chemical Society, Polymer Preprints, Division of Polymer Chemistry. Vol. 31 1. ed. Publ by ACS, 1990. p. 139-140.

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Liff, MIL, Lyu, PC & Kallenbach, NR 1990, Characterization of block oligomeric peptides by 2D 1H NMR. in American Chemical Society, Polymer Preprints, Division of Polymer Chemistry. 1 edn, vol. 31, Publ by ACS, pp. 139-140, Papers Presented at the Boston, Massachusetts Meeting of ACS 1989, Boston, MA, USA, 4/22/89.
Liff MIL, Lyu PC, Kallenbach NR. Characterization of block oligomeric peptides by 2D 1H NMR. In American Chemical Society, Polymer Preprints, Division of Polymer Chemistry. 1 ed. Vol. 31. Publ by ACS. 1990. p. 139-140
Liff, Mark I L ; Lyu, Ping chiang ; Kallenbach, Neville R. / Characterization of block oligomeric peptides by 2D 1H NMR. American Chemical Society, Polymer Preprints, Division of Polymer Chemistry. Vol. 31 1. ed. Publ by ACS, 1990. pp. 139-140
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